簡(jiǎn)要描述:低能電子散射/俄歇譜儀范圍內(nèi)的電子有很大的散射截面,因此背散射電子中絕大部分是被表面或近表面的原子散射回來(lái)的,這就使低能電子衍射(LEED)成為研究表面結(jié)構(gòu)的一個(gè)理想的手段。
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低能電子散射/俄歇譜儀
儀器簡(jiǎn)介:
晶體中的原子對(duì)能量在0~500 eV范圍內(nèi)的電子有很大的散射截面,因此背散射電子中絕大部分是被表面或近表面的原子散射回來(lái)的,這就使低能電子衍射(LEED)成為研究表面結(jié)構(gòu)的一個(gè)理想的手段。
Reverse View LEED
Reverse View LEED是世界上最早的商業(yè)化LEED裝置。經(jīng)過(guò)十余年的生產(chǎn)研發(fā)經(jīng)驗(yàn)的積累,Reverse View LEED已經(jīng)發(fā)展成為具有優(yōu)秀的性能、的穩(wěn)定性和豐富的軟件的LEED裝置,而且衍生出了一系列其它LEED型號(hào)。
低能電子散射/俄歇譜儀
● 電子束能量范圍0 ~ 3500 eV
● 可視角度達(dá)102度
● 可選配AES (Auger electron spectroscopy) 功能,能量分辨率好于0.5% FWHM ( Combination LEED and Auger control electronics with integral lock-in amplifier)
● 可選Video LEED對(duì)LEED圖形進(jìn)行采集和分析,以及I(V)、I(t)分析
● 可選W-Th燈絲或LaB6燈絲
MCP-LEED (Micro-channel plate control electronics)
MCP-LEED采用了高靈敏度的多通道板設(shè)計(jì),專(zhuān)門(mén)用于要求極低的一次電子束流的分析中,例如敏感材料、絕緣體等。
● 極低的一次電子束流,0.1 ~ 30 nA
● 最多兩級(jí)多通道板
● 可視角度達(dá)70度
● 極低的噪聲水平和*的穩(wěn)定性
LEED-AUGER OPTICS (Models BDL600IR and BDL800IR)
Glass-Display Fused silica glass coated with indium-tin oxide conductive layer and P31 phosphor ( ZnS:Ag:Cu-green, 525 nm wavelength)
BDL600IR......................... 90 angle of acceptance from sample at a distance of 50 mm
BDL800IR......................... 100 angle of acceptance from sample at a distance of 75 mm
Retarding Field Analyzer Concentric assembly of hemispherical grids
BDL600IR................ Working distance from sample 15 mm
BDL800IR................ Working distance from sample 18 mm
Grid Material.................. Gold coated tungsten wire mesh ( 100 mesh, 81% transparency)
Energy Resolution.......... 0.2% - 0.5% at low modulation volt.
Monitoring: 6” or 8” standard viewport
Linear Motion:Up to 150 mm retraction from sample (100mm standard); linear ball bearing and acme thread with all spring electr. connections
Integral Shutter : Open and close at any position of the linear motion
Magnetic Shielding : Mu-metal cylinder with front cover for maximum atteniuation
Assembly : Extreme-high-vacuum compatibility with stainless steel, high alumina and Au-plated copper alloy materials
Mounting : 6” (CF100) or 8”( CF150) double sided conflat flange with sample distance 145 mm -500 mm
Bakeability :Under vacuum, 250 C maximum
INTEGRAL MINIATURE ELECTRON GUN
Beam Energy : LEED - 5 eV to 750 eV
AES to 3000 eV
Beam Current :LEED - 2 uA at 100 eV and 0.5 mm beam size
AES - up to 100 uA at 3 keV
Beam Size :from 1 mm to 250 um - adjusted by wehnelt potential, limited by exchangeable aperture down to 50 um
Electron Source :Tungsten-2% Thoriated filament standard, single crystal LaB6 filament optional
Energy Spread :0.45 eV (tunsten-rhenium filament)
Overall Size : 10 mm lens diameter and 80 mm length
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